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梁珍惠,赖茂祥,刘华钢.HPLC法测定穿金益肝片中大黄素的含量[J].广西科学,2004,11(1):55-57. [点击复制]
- Liang Zhenhui,Lai Maoxiang,Liu Huagang.Determination of Emodin in Chuanjinyigan Tablets by HPLC[J].Guangxi Sciences,2004,11(1):55-57. [点击复制]
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| HPLC法测定穿金益肝片中大黄素的含量 |
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梁珍惠1, 赖茂祥2, 刘华钢3
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| (1.广西中医学院, 南宁市明秀东路 530001;2.广西中医药研究所, 南宁市东葛路 530022;3.广西医科大学, 南宁市滨湖路 530021) |
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| 摘要: |
| 用C18 ODS为固定相,甲醇-0.1%磷酸(85:15)为流动相,建立一种高效液相色谱法测定穿金益肝片中大黄素的含量,检测波长为290 nm。结果是进样量在0.05175~0.5175μg范围内线性关系良好(r=0.9998),平均回收率为98.56%,RSD为1.59%(n=5)。该方法简便,准确,重复性好,可作为该制剂的含量测定方法。 |
| 关键词: 穿金益肝片 大黄素 HPLC |
| DOI： |
| 投稿时间：2003-07-02 |
| 基金项目: |
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| Determination of Emodin in Chuanjinyigan Tablets by HPLC |
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Liang Zhenhui1, Lai Maoxiang2, Liu Huagang3
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| (1.Guangxi College of Traditional Chinese Medicine, East Mingxiulu, Nanning, Guangxi, 530001, China;2.Guangxi Institute of Traditional Medical and Pharmaceutical Sciences, Donggelu, Nanning, Guangxi, 530022, China;3.Guangxi Medical University, Binhulu, Nanning, Guangxi, 530021, China) |
| Abstract: |
| A HPLC method for determination of emodin in Chuanjinyigan tablets was established.A C18 Column was used with mobile phase of methanol -0.1% phosphoric acid(85:15) and the detection wavelength was 290 nm.The calibration curve of lincomycin was linear in the concentration range of 0.05175~0.5175 μg(r=0.9998).The average recovery was 98.56%(RSD=1.59%).The method is simple,accurate and reproducible.It is suitable for determination of emodin in Chuanjinyigen tablets. |
| Key words: Chuanjinyigan tablets emodin HPLC |
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