| 引用本文： |
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李俊,李甫,陆园园,张艳军,黄锡山.满山香子中水杨酸甲酯2-O-β-D-木糖基(1→6)-β-D-葡萄糖苷的分离与鉴定[J].广西科学,2006,13(3):217-218,225. [点击复制]
- LI Jun,LI Fu,LU Yuan-yuan,ZHANG Yan-jun,HUANG Xi-shan.Isolation and Identification of Methyl Salicylate 2-O-β-D-xylosyl (1→6)β-D-glucopyranoside from the Seed of Schisandra propinqua[J].Guangxi Sciences,2006,13(3):217-218,225. [点击复制]
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| 摘要: |
| 满山香子75%乙醇提取物的正丁醇萃取物,经大孔树脂柱色谱、Sephadex LH-20柱色谱、硅胶柱色谱和制备薄层色谱等色谱方法分离,得到1个糖苷类化合物,其化学结构经UV、IR、1HNMR、13CNMR、MS和元素分析确定为水杨酸甲酯2-O-β-D-木糖基(1→6)-β-D-葡萄糖苷。该化合物为首次从该植物中分离得出。 |
| 关键词: 满山香子 水杨酸甲酯2-O-β-D-木糖基(1→6)-β-D-葡萄糖苷 分离 结构鉴定 |
| DOI： |
| 投稿时间：2006-02-27修订日期：2006-04-06 |
| 基金项目:广西自然基金项目(桂科自0339032)资助 |
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| Isolation and Identification of Methyl Salicylate 2-O-β-D-xylosyl (1→6)β-D-glucopyranoside from the Seed of Schisandra propinqua |
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LI Jun, LI Fu, LU Yuan-yuan, ZHANG Yan-jun, HUANG Xi-shan
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| (Department of Resource and Enviromental Science, Guangxi Normal University, Guilin, Guangxi, 541004, China) |
| Abstract: |
| The n-butanol extracts of the seed of Schisandra propinqua (Wall)Hook.f.et Thoms.were separated with column chromatography of macro-porous adsorption resins, Sephadex LH-20, silica gel and preparative thinlayer chromatography.One compound was obtained and its structure is identified as methyl salicylate 2-O-β-D-xylosyl (1→6)β-D-glucopyranoside on the basis of UV, IR, 1HNMR, 13CNMR, MS spectroscopic analysis and element analysis.The compound is isolated from this plant for the first time. |
| Key words: seed of Schisandra propinqua methyl salicylate 2-Oβ-D-xylosyl (1→6)β-D-glucopyranoside isolated structure identify |
