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  • 黄建猷,卢文杰,谭晓,陆国寿,黄周锋.中平树根部脂溶性成分的GC-MS分析[J].广西科学,2015,22(2):153-155.    [点击复制]
  • HUANG Jian-you,LU Wen-jie,TAN Xiao,LU Guo-shou,HUANG Zhou-feng.Analysis of Liposoluble Components from Macaranga denticulata (Bl.) Muell.-Arg.by GC-MS[J].Guangxi Sciences,2015,22(2):153-155.   [点击复制]
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中平树根部脂溶性成分的GC-MS分析
黄建猷1, 卢文杰1,2, 谭晓1, 陆国寿1, 黄周锋1
0
(1.广西中医药研究院, 广西南宁 530022;2.广西中药质量标准研究重点实验室, 广西南宁 530022)
摘要:
[目的]研究中平树根部的脂溶性化学成分,为其药用资源的进一步开发利用提供科学依据。[方法]采用硅胶柱层析法对脂溶性成分进行分离,甲酯化后再通过气相色谱-质谱-计算机联用技术对其进行分析和鉴定。[结果]分离出30个组分,确认了其中的21个成分。[结论]分离得到的脂溶性成分主要为脂肪酸类化合物,所有成分均为首次在该植物中分离鉴定出。
关键词:  中平树  气相色谱-质谱-计算机联用技术  脂溶性成分
DOI:10.13656/j.cnki.gxkx.20150401.005
投稿时间:2014-09-13修订日期:2014-10-15
基金项目:广西中药质量标准重点实验室系统性研究课题(桂中重系201307)资助。
Analysis of Liposoluble Components from Macaranga denticulata (Bl.) Muell.-Arg.by GC-MS
HUANG Jian-you1, LU Wen-jie1,2, TAN Xiao1, LU Guo-shou1, HUANG Zhou-feng1
(1.Guangxi Institute of Traditional Medical and Pharmaceutical Sciences, Nanning, Guangxi, 530022, China;2.Guangxi Key Laboratory of Traditional Chinese Medicine Quality Stardands, Nanning, Guangxi, 530022, China)
Abstract:
[Objective] The liposoluble components from Macaranga denticulata (Bl.) Muell.-Arg.were studied in order to provide the scientific basis for the further development and utilization of this medicinal resource.[Methods] Liposoluble components from Macaranga denticulata (Bl.)Muell.-Arg.were isolated by silica gel column chromatography, and then the isolated liposoluble components were analyzed by GC-MS-DS technique after methyl esterification.[Results] 30 components were separated and 21 of them were identified.[Conclusion] Fatty acids were major chemical constituents of these liposoluble components.All the compounds were isolated and identified from this plant for the first time.
Key words:  Macaranga denticulata (Bl.) Muell.-Arg.  GC-MS-DS  liposoluble components

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