窿缘桉叶和果实的挥发性成分分析

Determination of Volatile Constituents in Leaves and Fruits of Eucalyptus exserta

关键词:  气相色谱-质谱联用  窿缘桉  挥发油  成分分析

Key words:  GC-MS  Eucalyptus exserta  volatile oil  composition analysis

摘要:

[目的]利用GC-MS对窿缘桉叶、果实的挥发性组分进行定性定量分析。[方法]采用水蒸气蒸馏法分别从窿缘桉叶、果实中提取挥发油,用乙醚作为溶剂从蒸馏残液中萃取水溶性挥发组分。[结果]窿缘桉叶得油率为0.95%(以鲜质量计),其中挥发油主要成分为桉叶素(38.82%)、α-蒎烯(13.52%)和对伞花烃(12.04%);其蒸馏残液中的水溶性挥发成分主要物质为(1R,2R,3S,5R)-(-)-2,3-蒎烷二醇(14.75%)。果实得油率小于叶,为0.52%(以鲜质量计)。果的挥发油成分主要为β-石竹烯(13.07%),其蒸馏残液中的水溶性挥发成分主要为α-松油醇(25.33%)。[结论]窿缘桉果实挥发油的油相成分中含有大量石竹烯,作为药物原料具有天然优势。

Abstract:

[Objective] The volatile components of Eucalyptus exserta leaves and fruits was analyzed by GC-MS.[Methods] By the way of steam distillation, volatile components was extracted from the leaves and fruits of Eucalyptus exserta.The water-soluble volatile component was extracted from the distillation residual solution with Diethyl ether as a solvent.[Results] The extraction yield of essential oils from the leaves was 0.95% (on fresh weight basis).The major constituents of essential oils were Cineol(38.82%), α-Pinene(13.52%) and p-Cymene(12.04%).The main substance in water-soluble fraction of the distillation residual solution was (1R, 2R, 3S, 5R)-(-)-2, 3-Pinanediol (14.75%).The oil yield of fruits was less than leaves, and it was 0.52% (on fresh weight basis).The major constituents of essential oils of fruits was Caryophyllene (13.07%), and the water-soluble fraction was α-Terpineol (25.33%).[Conclusion] The results could provide a reference foundation for improving the comprehensive utilization of Eucalyptus exserta.